NMR Facility
Training
To use the instruments, one must attend a training class and be issued a computer login with password. If you are interested in attending a training session, please contact facilities supervisor Russ Hopson.
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Russell Hopson
NMR Facility Supervisor
Reservations
Reservations for the NMR spectrometers can be made via the Faces Scheduling System.
Names and Locations of NMRs
Name | Location | Probe | Best NMR for |
---|---|---|---|
ZEUS |
GC410 - 400MHz Furthest from Door on Left |
z-BBO |
2nd most sensitive for all nuclei |
ARTEMIS |
GC410 - 400MHz Closest to Door on Left |
z-BBFO |
2nd most sensitive for all nuclei |
CRONUS |
GC410 - 600MHz Closest to Door on Right |
z-BBFO |
Most sensitive for all nuclei |
NOTE: A 10ul Capillary NMR probe and an 4mm HR-MAS probe are available for the 400MHz spectrometers and can be installed upon request. A 600 MHz z-BBO that can lock on 19F on the 1H channel, and observe 2H on the BB channel, as well as a z-TXI probe are available for the 600 MHz Spectrometer.
Guides & Resources
- How to setup and acquire a 1-D 1-H and 13-C NMR with Topspin
- Quick guide to changes on Artemis - 9/2020
- How to measure T1
- How to measure T2
- How to setup and aquire COSY experiments
- How to setup and acquire HMQC or HSQC experiments
- How to setup and acquire HMBC experiments
- How to setup and acquire NOESY experiments
- How to setup and acquire a 1-D TOCSY
- How to setup and acquire Diffusion Experiments
- How to setup and acquire using Solvent Suppression
- How to Observe 19-F on ARES
- How to Observe 2-H NMR
- How to use the CapNMR Probe
- How to run the ICONNMR
- How to perform variable temperature experiments
- Brown NMR Facility Magnet Specs
- Magnet Safety Documentation
- Saving NMR data to USB Drives
- Saving NMR by SSH
- Transferring Files
- How to obtain and set up free Topspin processing software
- NMR processing software is available from MESTREC.
- Introductory NMR Lecture
Contact Information
For queries regarding the facility, equipment and other related questions, please email Russell Hopson, Ph.D., NMR Spectrometer Specialist.
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Russell Hopson
NMR Facility Supervisor